Monday, August 15, 2016

Sulfur of Saturn

The Roman Goddess Ops, 'sweet'-heart (and wife)
of Saturn, Peter Paul Rubens c. 1630,
“Abundance (Abundantia).” [1]
Antonio Neri’s book on glassmaking, L'Arte Vetraria, devotes an entire chapter to making artificial gems. These are made with an especially dense, refractive form of lead glass—what today would be called lead crystal. He made it in small batches, in sealed ceramic vessels; each infused with various metal oxide pigments to give characteristic jewel tone colors.  His secret ingredient for making the finest artificial gems was a material known as "sulfur of Saturn." He writes:
You will have jewels of marvelous beauty in every color, which by far surpass those described above, made with ordinary minium. Because with this true sulfur of Saturn, they will surpass all others by far more than I can write here, as I have seen and made many times in Antwerp.[2]
This "ordinary minium" that he speaks of is one of several oxide forms of lead, also known as 'red lead,' it is bright red or orange in color. As a stable red pigment it was well known to ancient Byzantine and Persian illuminators. [3] It was so popular, in fact, that the word used to describe small intricate pictures 'miniature,' is derived directly from 'minium.' [4] The intricate embellishments in manuscripts ultimately took on the name of the scribes' favorite color.  In glass, minium does not impart red or any other color on its own, but does add 'sparkle' and made Neri's jewels highly refractive to light. 

In the recipe, he uses white vinegar and he reacts it with finely ground minium through a laborious process. The acetic acid in vinegar chemically combines with the minium to form lead acetate, which alchemists called "sugar of Saturn" because it had a distinctively sweet taste (more on that later). [5] Lead (Saturn) could be added to the melt in a number of different forms including acetate, carbonate and various oxides. The heat of the furnace reduces them all and the result is essentially identical glass from any of these sources. The lead acetate has one major advantage that set it apart from the others. Lead acetate is soluble in water and therefore it can easily be purified of contaminants and to a much higher degree. It can be filtered, allowed to stand and decanted after any insoluble impurities settle out.

In other references "sugar of Saturn" and "sulfur of Saturn" are considered synonyms. This is not the case with Neri, for him they are two different substances; the 'sugar' is a precursor for his final product, sulfur of Saturn:
Left in the bottom will be a salt as white as snow, and as sweet as sugar. Repeat the dissolution, and filtering, and evaporation with common water three times. This is the required sugar of Saturn. 
Keep it to calcine in sand in a glass flask or ball in a furnace over a moderated fire for many days. It will further calcine to a color that is much redder than cinnabar, and more finely impalpable than sifted grain flour. This is the required true sulfur of Saturn; purified from the sediment, foulness and blackness that were upon the lead at first. [6]
It would be a reasonable guess that by heating the acetate for "many days" he is reducing it back to minium, its more basic, bright red oxide state, but this time in a greatly purified form.

Unfortunately for his health, in this recipe for sulfur of Saturn, Antonio makes extensive use of heating and evaporation. Even more unfortunate is that in a number of steps he judges the potency of his product by taste. Lead acetate is highly toxic; because it is soluble in water, it enters the bloodstream easily. It attacks the nervous system, accumulates in the bones and can cause organ failure. It is quite likely that by breathing the fumes and tasting crystals of sugar of Saturn, Neri was contributing to his own demise at the relatively young age of thirty-eight. Lead acetate was not the only toxic substance he handled regularly, but it was certainly one of the worst for his health. 

 It does not follow that he was totally ignorant of the risks he was taking. The dangers of heavy metals were recognized from early times. Pliny speaks of the noxious fumes from lead furnaces, and Plutarch opined that lead and mercury mines were "unwholesome and pestilent places." Neri’s own father followed the work of Dioscorides, who wrote that ceruse (lead carbonate), taken internally, could be fatal and that certain sweet wines could adversely affect the abdomen and the nerves.

Ancient Romans discovered that when wine started to turn to vinegar, it could be boiled down in lead lined pots to produce a highly sweet syrup called sapa. A late Roman cookbook made extensive use of sapa, which presumably contained considerable lead acetate. [7] It has been conjectured that  lead laced sapa contributed to poisoning among the Roman aristocracy. While lead acetate is a deadly poison, it is a step too far to imply that it contributed to the fall of the Roman Empire.

[1] Alchemical tradition does provide for an association between the metal lead and the Roman god Saturn. However, there is no such association between 'sugar of Saturn' and either of his consorts Ops or Lua, although Ops, the goddess of abundance (opulence) does rather nicely represent the chemical that made Neri's most opulent artificial gems possible.
[2] Neri 1612, ch. 91.
[3] Chemically, this is Pb3O4, also known as Lead (II,IV) oxide, triplumbic tetroxide. Historically, it was called minium and red lead.
[4] The accepted etymology of ‘miniature’ is from ‘minium,’ but may have been influenced by similar Latin terms such as  minor, minimus, minutus, etc.
[5] Lead acetate comes in two forms; Pb (C2H3O2)4 and Pb (C2H3O2)2, both are toxic; the later variety is soluble in water.
[6] Neri 1612, ch. 91.
[7] “Saba” endures today as a popular grape syrup, albeit without the lead.


* This post forst appeared here on 12 September 2014.

Friday, August 12, 2016

Alberico Barbini

The island of Murano , circa 1600
attributed to Danckerts
In the early seventeenth century, Antonio Neri began preparing batches of glass for the royal family in Florence, Italy. This was a specialist vocation undertaken by alchemists, which by schooling, Neri was. His job as “conciatore” involved procuring the ingredients, preparing, mixing and melting them and working with the glass artisans, adjusting the consistency and colors for the work being done. It was a position that carried great prestige, and Neri’s book on glassmaking [1] would cement his name in history. 

Shortly before Neri was born, in 1576, the grand duke of Tuscany, Cosimo I de’ Medici, brokered a special deal with the doge of Venice to have master glass artisans come to Florence and teach their secrets. These men were from the island of Murano; the most famous center of glassmaking anywhere. There is only scant evidence that Neri himself traveled to Venice and perhaps only once, but there is no doubt that he benefited greatly from the knowledge of Muranese workers in Florence, Pisa and Antwerp during his lifetime. 

Over the intervening centuries, the title of the glass batcher changed, but the tradition and prestige of glass formulation continued well into the middle of the twentieth century. In fact, even today, among the small glass manufacturers that compose the studio glass movement, the glass batcher is considered to be something of a modern alchemist; keeper of the arcane knowledge of  the chemicals and amounts necessary to produce special colors and adjust properties of the glass.

Now, fast forward four centuries from Neri's Italy; in the early 1920s, a Milanese lawyer named Paolo Venini partnered with a Venetian-born antique dealer friend, Giacomo Cappellin, to start a new glass factory on Murano. [2] Even as recently as this, the glass batcher still held a respected position both within the factory and the community. Through several incarnations over the next half century Venini grew a world-wide reputation for innovative designs, of which color played an important part. They are specifically associated with the fazzoletto (handkerchief) style vase and the incalmo technique of fusing two or more colors of glass seamlessly in a single furnace-blown piece. 

In 1925, Cappellin split from Venini and took many of the craftsmen with him, in 1933 the new business was acquired by Pauly & C. Again, chemical knowledge and the artistry of reproducing ancient colors made a worldwide reputation. [3] As ownerships changed hands like cards in a game of poker, artisans shuffled between factories. It is easy to lose track of the individual glassworker. Even for a period so recent, many records exist only in the heads of the family members still living on the island. 

In 1956 the Stazione Sperimentale del Vetro (Experimental Station for Glass) was started on Murano with the mandate to preserve and promote the technical aspects of Italy’s glassmaking heritage. [4] The new institution was regarded by some traditionalists with great suspicion, but as we will see, others embraced the resource.

I recently sat down with renowned glass artist Emilio Santini, who today carries on a six-centuries-old family tradition in glasswork. [5] Emilio had recently called home, to Murano, which led to his father’s recollection of an uncle, who worked making color for Venini and Pauly. Here Emilio recounts the conversation:
Alberico Barbini was the uncle of my father, Mario Santini and the man in charge of making the glass batch “partie” (Venetian) “partite” (Italian). He was the brother of my grandmother, Delfina Barbini. He was not the only one [in my family] who worked for Venini in the early days but the most respected. At Venini he worked formulating glass after another great batch maker, [Albino] Carrara. 
In the early to mid [twentieth] century the batch maker still held an important position in the factory, not like now, you know, and he kept his formulations quite secret, although this relative of mine, Alberico, was smart enough to use the most modern technology available at that time. 
He was different from other batch makers in that when the Stazione Sperimentale del Vetro opened, he made extensive use of it in reproducing colors. At that time, and even now to an extent, the institution was not seen as good for traditional Murano glassmaking. 
He later moved on to Pauly where he was in charge of reproducing the glass colors that were in use in the seventeenth, eighteenth and nineteenth centuries. First, he assisted in remaking broken or missing pieces in private collections, then later in making reproduction antique stemware at Pauly that was impossible to distinguish from the originals. 
You must realize that all this does not come from documents but from the memory, still very sharp and lucid, of my father.
Addendum: On 7 August 2016, at the age of 96, Mario Santini died, surrounded by his family at his home on Murano.


[1] L’Arte Vetraria, (Neri 1612).
[2] Paolo Venini http://en.wikipedia.org/wiki/Paolo_Venini also see https://www.facebook.com/pages/Venini/198475426829887
[3] Pauly & C. Compagnia Venezia Murano http://en.wikipedia.org/wiki/Pauly_%26_C._%E2%80%93_Compagnia_Venezia_Murano
[4] Stazione Sperimentale del Vetro  http://www.spevetro.it/indexENG.htm
[5] Emilio Santini http://www.cmog.org/bio/emilio-santini
* This post first appeared here on 25 Feb 2015.

Wednesday, August 10, 2016

Sal Ammoniac

Alchemical symbols used to denote sal ammoniac.
Today we will examine "sal ammoniac," a common alchemical ingredient used by Antonio Neri in many of his preparations. In its pure form, it is a colorless crystalline material and is known to chemists as ammonium chloride. It does occur as a (rare) natural mineral, but it was also manufactured as early as the thirteenth century, as noted by alchemist Albertus Magnus in his De alchymia.[1] Neither he nor Neri provides a recipe for sal ammoniac, but other sources indicate that it was made by allowing urine to putrefy with common salt. French investigators documented another method used in Egypt in the eighteenth century. This scheme involved burning the dung of animals who fed on spring grasses and then sublimating the ammoniac out of the resulting soot. Sublimation occurs when a heated material goes directly from a solid to a gaseous state without ever becoming liquid. Sal ammoniac has this property; when heated it turns to a gas and upon cooling, turns back to a solid.
Sal Ammoniac,
natural formation

The usefulness of sal ammoniac in alchemy stems from the fact that when dissolved in water, which it does easily, it immediately dissociates into equal parts of ammonia and hydrochloric acid, which in turn will dissolve some metals, including tin, zinc, iron and (reluctantly) lead. Its most famous use was as an additive to the stronger acid aqua fortis (nitric acid). Together the two formed aqua regis which was strong enough to dissolve gold. At the time that Neri was working, the only known way to dissolve the most 'noble' of metals (gold) was with the 'king' of acids (aqua regis). Neri puts this knowledge to use in his recipe for ruby-red colored glass made with pure gold. His description is light on details, but he does clearly direct the reader to dissolve the precious metal in aqua regis, then gently evaporate away the acid to obtain the red pigment.

Elsewhere in Neri's glassmaking book, L'Arte Vetraria,[2] he uses sal ammoniac in the production of "alemagna blue" paint and in the tinting of natural rock crystal. 

Another of Neri's creations requiring sal ammoniac was Chalcedony glass. It had swirls of every color the glassmaker could produce. He achieved this feat by making extensive use of aqua regis to dissolve each of a long list of metals. He then gently evaporated off the acid, leaving ultrafine powdered metals, which he added as pigments to the glass melt. 
With this powder, I made a chalcedony in a glass furnace in Antwerp that was then run by a most courteous gentleman; Mr. Filippo Gridolfi. This chalcedony gave rise to work so nice and graceful, that it emulated true oriental agate, and in beauty and delightful colors by far exceeded it.
Today, chemical factories produce vast quantities of the materials used by Neri in his glassmaking exploits and in far higher purities. Having unlimited quantities of every conceivable chemical compound at our fingertips makes it difficult to appreciate the physical labor involved by seventeenth century alchemists, both in the preparation of the glass and in the production of the individual ingredients. The chalcedony glass recipe cited above must have taken workers many, many hours to produce and must have cost a small fortune. 

[1] Magnus 1958.
[2] Neri 1612.
[3] Glauber and others used the term 'sal ammoniac' to describe a related chemical (NH4)2SO4. When mixed with aqua fortis this forms a nitric-sulfuric acid solution, which does not form aqua regis, and does not dissolve gold.
* This post first appeared here on 22 August 2014.

Monday, August 8, 2016

Alchemy School

Frontispiece woodcut from
 De Chemia Senioris, by Zadith ben Hamuel, 1566
A common notion holds that alchemists were eccentrics, lone practitioners working in dingy basements, cut off from the rest of the world. This was a myth already well established in glassmaker Antonio Neri's time, but far from the whole truth. In the early seventeenth century, alchemy was practiced in medicine and pharmacy, in precious metals refining and even in the preparation of artists' supplies. The glassmaker was in good company. Where Antonio Neri received his training is unknown, but there are intriguing clues.

We turn first to Antonio's own father, Neri Neri, the royal physician to the Medici family. According to historian Giulio Negri, he received his medical degree at the prestigious Studio Fiorentino, the forerunner of today's University of Florence. At the time, it had already been in operation for two centuries, having been granted a charter in 1348 by Holy Roman Emperor Charles IV. The charter was a response to a personal appeal by Archbishop Piero Corsini. Antonio Neri's own distant relative, Ser Giovanni Neri, later became Corsini's secretary, so a family legacy of attendance is not out of the question. That our priest might attend his father's alma mater is pure speculation, but it seems foolish to doubt that he started his alchemy education at his father's knee, in his own home.

The manuscript entitled Treasure of the World that Antonio devoted to "all of alchemy" was completed in 1600, but started two years earlier. On a page near the beginning, dated 1598, the twenty-two year-old clearly identifies himself as a "priest." Church rules forbade anyone from becoming a novice before the age of sixteen, which for Neri would have been in the spring of 1592. Full ordination as a Catholic priest typically took six years, meaning in 1598 Neri only recently underwent the 'laying on of hands' ceremony by the archbishop, confirming his title. The inescapable conclusion is that Neri learned his craft while in seminary and the Church sponsored his education. 

The identity of Neri’s order is a mystery, but the few scattered pieces of the puzzle that we do have allow for some interesting speculation. The list of candidates having some connection to the priest and the means to support, if not supply an education is not long. The five names that stand out are the Dominicans, the Carmelites, the Augustinians, the Knights of Malta and the Benedictines. The Dominicans were noted for their scholarship and ran two apothecaries in Florence. The Carmelites are named in the deposition notes taken by Agnolo della Casa, which identify Neri’s confessor as such. The Augustinians counted a Francesco Neri as abbot of their San Clemente monastery who worked for Don Antonio de’ Medici at the Casino in 1619. Antonio’s aunt, Faustina, apparently entered an Augustinian convent after the death of her husband.  Also, though Neri’s confessor was a Carmelite, he also served as the parish priest of an abbey run by the Canons Regular of the Lateran—an independent Augustinian congregation. The Knights of Malta ran two churches in Florence and Neri can be connected to both.  The knights followed the rule of Augustine and enjoyed a close relationship with the Augustinians. The order traces its roots to the crusades  and has various associations with alchemy such as George Ripley. Their main presence was on Malta, though in 1565 they suffered a devastating defeat there to the Ottomans. Neri was not a knight, but he could have occupied a place in their clergy. In Florence, any resources for schooling in alchemy by the knights would have been overseen by its most prominent local official; that official was Neri’s benefactor Don Antonio de’ Medici, Grand Prior of Pisa. The Benedictines were also associated with Neri’s family and had the means to provide him with an education in alchemy. He was born in the parish district of Benedictine church, San Pier Maggiore. His father was buried in the Cistercian (reformed Benedictine) church of Cestello. His sister  committed to a Benedictine order (the Camaldolese). After his ordination, in 1601, Priest Antonio Neri lived across the street from the Vallombrosan (Benedictine) mother church, Santa Trinita.

In any case, as royal physician Neri's father was an esteemed member of the court and Antonio would have enjoyed rare access to its inner sanctum. The grand duke's own laboratory at the Galleria dei Lavori certainly would have been a familiar haunt for our alchemist-priest.

This post first appeared here in a shorter form on 2 October, 2013.

Friday, August 5, 2016

Filippo Sassetti

Goa, India 1509
In the Florentine baptism records, the entry for Antonio Neri was made on a Thursday, the first of March, 1576. He was born the previous evening, to Dianora Parenti and Neri Neri. His godmother is listed in the document as Ginevra Sassetti. Not a great amount is known about her; she was from a prominent family, at the time in her late fifties. However, there are indications that other members of her family interacted with the Neri's. Her nephew Filippo mentions Antonio's father favorably several times in letters, providing a fascinating glimpse into the way disease was diagnosed and treated.

When Antonio was born, his father Neri Neri was in his early thirties, and already a highly regarded physician. Baccio Valori was director of the famed Laurentian Library in Florence and steward of the Medici's simples (medicinal herbs) garden. He was friend to Neri Neri and godfather to Antonio's oldest sister Lessandra. Between 1583 and 1588, Valori received letters from a mutual friend, Filippo Sassetti, who was living in Goa and Cochin – trading settlements in India. Filippo was a native Florentine; he attended university in Pisa with Valori and they became lifelong friends. After Sassetti's father was forced to sell the family home to pay off a debt. Filippo moved to Lisbon and became a spice trader. Not suited for a desk job, he soon set sail seeking adventure in the orient. 

In a 1586 letter to his old friend Valori, Sassetti discusses an Indian remedy against the plague, with a substance called bezoar. The bezoar stone is a mass that develops and becomes trapped in the digestive systems of certain animals. It often resembles a smooth rock. Some thought ground bezoar to be a universal antidote to any poison. Sassetti was puzzled about how the grindings of bezoar could work to cure the plague. Its Aristotelian elemental properties would not be a match for correcting the imbalance of humors in the body. "This is a principle," he explains, taught to him by Neri Neri. "I have thought about it and I can not understand how it works, because the plague is of the same corruption and this is a lack of heat inherent in the humidity. And the stones, if I recall correctly, they have a cold and dry complexion, hence may not precede the restoration of heat. Messer Neri one time did me the favor of telling me." 

In another letter to Baccio Valori, Sassetti notes that he has collected rare varieties of cinnamon in his travels along the Malibar coast in India. His intention was to rediscover the species thought to be a powerful cure of disease by the ancients. He planned to send a parcel of seeds of these and other medicinal plants. "If it pleases God, in the coming year, I will send this to you, so that you may see it all, together with our Messer Neri Neri, who graces my memories." Later he writes that he is sending Baccio the discourse on cinnamon, which he has compiled, along with some plants. These, it later turned out, were water damaged in the journey. He had hoped for some help from Neri Neri on the question of whether the cinnamon he collected from the island of Zeilan [Ceylon], is the same thing as the curative cinnamon of Mantua described by the ancients. Valori was an authority on these matters in his own right. As librarian for the Medici's imposing collection of books and manuscripts, he had vast academic access. As keeper of the simples garden, he had first hand experience in horticulture and its derivative medicinal cures. 

The principles of "humorism" were passed down from celebrated physicians of the ancient world, like Galen, Hippocrates and Dioscorides. It was thought that the cure of disease was dependent on the restoration of balance between four substances in the body: blood, phlegm, black bile and yellow bile. In turn, each of these was associated with one of the Aristotelian elements: air, water, earth and fire respectively. Each was further associated with specific symptoms and characteristic traits of the patient, even their psychological outlook and physical complexion. This system formed the foundation of Western medicine and was taught and practiced well into the nineteenth century. Although, within Antonio Neri's lifetime newer experimentally based methods did start to take hold. A decade after his father's death, in a 1609 letter, Antonio boasts about his success in curing disease in Antwerp using the methods of the medical upstart Paracelsus. It is unlikely that his father would have approved.

*This post first appeared here 13 August 2014.

Wednesday, August 3, 2016

Crocus Martis

The many different alchemical symbols used to denote crocus martis.
In order to understand the seventeenth century glass recipes of Antonio Neri and for that matter, any alchemical recipes, it is first necessary to have a grasp of the chemical repertoire. The ingredients referenced by Neri were not especially exotic, but over the intervening four centuries since he wrote, the common names of materials have changed considerably. In the current lexicon, we name materials by their chemical formulas, so iron oxide names its two constituent elements, iron and oxygen. But in the seventeenth century, the periodic table of elements was a concept yet to be invented; hence "crocus Martis." Martis refers to Mars, the Roman god of war, the red planet, and the ancient alchemical name for iron. The origins of crocus are lost, but it may refer to the similar looking spice saffron, (crocus sativus) which has been highly valued since antiquity; poetically, 'saffron of Mars'. 

A first encounter with the technical recipes of sixteenth and seventeenth century alchemy can be confusing, frustrating and more than a little disorienting. There is no shortage of records, letters, manuscripts and recipe books that have been preserved from that period, however, the challenge lays in making sense of them in a way that relates to our current view of the world. It is understandable that alchemical materials and compounds had unfamiliar names; but even larger difficulties arise with the realization that any given name might describe several different chemicals, and in fact, there may be several different interchangeable synonyms/symbols for any given name. As it happens, there were good reasons for this state of affairs and taking the time to understand them really opens up a window onto a strange and wonderful landscape of history. 

Antonio Neri considered himself an alchemist first and glassmaker second. His purely alchemical works are somewhat cryptic, but in the glass book he bends over backwards to be accessible to novices. Because of this crossover, his work can help us to navigate details in both areas that might otherwise go without explanation. His writings broadly divide into two categories: one intended for generally curious readers and another intended only for those familiar with the arcane coded language of alchemy. We have examples of both styles by Neri and all written within the period of about fifteen years at the beginning of the seventeenth century. As a result, we can use his works intended for a general audience to decode some of his more arcane passages. With the glass recipes, his careful explanations lead us to gain considerable confidence in his technical abilities. In the introduction to his famous book on glassmaking, L'Arte Vetraria, he wrote, "I have described every last detail clearly and distinctly in this work, I am sure that if you do not purposely foul up, it will be impossible to fail, after having acquired experience and practice." Even in Neri's more obscure works, he earned the respect of later chemists; in 1870, in the journal Nature, George Rodwell, the first science master of Marlborough College, pronouncing him a "sensible chemist." Rodwell went on to note that Neri had used "no less than thirty-five different names, and twenty-two symbols" to denote a single material, the metal mercury. 

In still other writings, it becomes clear that Neri was deeply concerned that some alchemical operations were inappropriate for general consumption and were better kept secret among true practitioners of the art. In particular, he worried that if the transmutation of base metals into gold and silver were practiced widely, the result would be a collapse of the economy and would ultimately plunge civilization into disarray.

We will start with his glass book, where his materials and methods are detailed with special consideration for those not familiar with the art. Then perhaps we can build on that and make sense of his more esoteric material.

In L'Arte Vetraria, Neri gives four different methods to make crocus Martis. He explains: 
Crocus Martis is nothing other that a refinement and calcination of iron. A means by which its pigment, that in glass is a deep rutty red, is opened and imparted to the glass. It not only manifests itself but makes all the other metallic colors as well, which ordinarily hide and are dead in the glass, dance in resplendent apparition. Since this is the way to make the hidden metallic colors appear, I have put down four ways to make it.
The term calcination means only 'to roast' in a hot oven. It derives from the ancient practice of cooking seashells into powdered quicklime, which is a prime ingredient of cement; now called calcium oxide.  In his first method for crocus Martis, Neri mixes iron filings with sulfur and then heats the mixture in the furnace for a long period. We can guess that the result is a mix of iron oxide and iron sulfide. These are the constituents of a popular red pigment of the same name (crocus Martis) used in pottery glazes. In the second method, he takes the iron and sulfur mixture and sprinkles it with vinegar and leaves it in the sun for many days. The third method uses aqua fortis (nitric acid) for better effect. In the fourth and final method, Neri uses aqua regis, an even stronger acid. 

In all four cases the predominant result will be for the acids to chemically react with the metal to form iron oxide and sulfide, but alas, chemistry is not that simple; there will be minor concentrations of other compounds depending on the acid used, which may or may not affect the final product. We must consider that vinegar and the other acids in the seventeenth century were significantly different from those products today. They were made by different methods and contained a variety of impurities that would never be found in the current products. As Neri notes, each method produces different effects in the glass and therefore we must conclude that each, to some extent, differs in chemistry as well. Today, we know that iron forms several different oxides, each responsible for different color effects in glass. In a number of green glass recipes Neri uses crocus made with vinegar, yet in chapter 71 he uses it to diminish the green in yellow lead crystal. In chapter 124 he uses crocus made with aqua fortis for red glass. The lesson here is that the name of a material tells us only the basics, how it was made is at least as important if not more so. 

* this post first appeared in a somewhat different form on 15 August 2014.

Monday, August 1, 2016

Reports From Parnassus

Rafael - El Parnaso (Vatican, Rome, 1511)
Apollo on Parnassus, (fresco detail). 
In the spring of 1612, Italian glassmaker Antonio Neri finished writing L’Arte Vetraria, and the Holy Office of the Inquisition approved it for publication. The book of glass technical recipes passed the Church’s censors despite it containing a large number of alchemy related methods. Contrary to what we might imagine, they did not have any problems with Neri’s work; in fact, one bureaucrat commented that the book was full of useful information. Remember, this was at the same time that so-called sorcerers and witches were being tortured and executed around Europe. One big difference in this case was intent, or rather the perceived intent of Neri's writing. Another factor was his personal connections. The truth is that alchemy was something of a fad among the wealthy nobility, who used the equipment for everything from making rosewater, to distilling liquor, to quietly trying their hand at transmutation. 

To form a better sense of the public image of the chemical arts in the early seventeenth century, we can turn to the satirical critic Traiano Boccalini, who published a book of his own the same year as Neri. Ragguagli di Parnaso [Reports from Parnassus] was an immediate hit. In fact, it became so popular that he and his sharp tongue were forced to leave Rome for the comparative safety of Venice soon after its completion, and soon after that friends found him dead under suspicious circumstances. Initially, Boccalini had been on good terms with Church officials, but perhaps he had seen a bit too much of the inner workings of the ChurchEventually, he became bitterly disillusioned and wrote Ragguagli as a collection of fictitious news-sheets. These were patterned after the letters that circulated widely as the forerunners of modern newspapers. His reports took place in the mythical state of “Parnassus,” which struck an uncanny resemblance to contemporary Rome. Its monarch, Apollo, struck an uncanny resemblance to the pope, as the princes of Parnassus did to cardinals, bishops and curia officials. Report LXXXIX is illustrative of what were the more practical fears over alchemy, in this case, some creative wealth building among the clergy. It gives a sense of alchemy’s public persona. Apparently, in real life, there was a crackdown by the Church on chemical apparatus, under the guise of concern for public health. Our author slyly suggests, in the very last line, that it may have had more to do with putting an end to clergy lining their own pockets. 
Apollo [the pope] Prohibits the Princes from the Use of Distillers or Alembics At Home: 
In the past few months here, various ailments have emerged in this state of Parnassus, which have caused in some an extraordinary fatigue with frequent agitation: in many a tenacious fever, a faint pulse and a monstrous appetite: in others an intense stomach ache with an ardent thirst.  
The doctors cannot find a single remedy. However, the true cause of these maladies, by decree of Apollo, was revealed before a recent meeting of the grand Asclepius [Society] of prominent Greek, Latin and Arabic doctors, where it was the subject of long and erudite debate. Because neither the enemies of the grand princes nor other eminent gentlemen were spared, it was doubted whether the sickness was caused artificially by powerful poisons. Furthermore, it is clear these troubles were not only happening nearby.  
And we see several modern princes put great study in their most excellent facilities to prepare in their alembics things other than rose water. They conceal subjects dangerous and heinous with their hidden machinations of poison. This cannot be allowed to be covered up; such a scandal must be exposed with the violence of a dagger.  
His Majesty, concurring with the opinion of the congregation, yesterday morning made a public speech, to issue a strict edict, which forbids princes of any color, from ever keeping distillation or alembic operations at home or outside. However, he allowed similar exercises in the hands of experimenters and herbalists. A thing being extremely foul is the minting of counterfeit money in the night and then by day covering so treacherous a crime by running shops openly making medals for the crown. 

In this piece, Boccalini crystallizes the complex social stigma carried by alchemy. Of all the practical tasks that could be performed in this art, the most notoriety by far was derived from the concept of turning base metals into gold. In his writing Neri openly expressed his fear that true transmutation, in the hands of the masses was likely to collapse the economy. The Vatican’s concerns were more immediate: financial gluttony within the Church. Anyone with enough alchemical knowledge could produce convincing counterfeit money. Turning lead into gold was a theoretical issue; dealing with rogue counterfeiters was a real and immediate one. 

*This post first appeared here on 8 August 2014.