Showing posts with label Palladium spagyricum. Show all posts
Showing posts with label Palladium spagyricum. Show all posts

Friday, July 3, 2020

Glass of Montpellier

Montpellier, France, in the seventeenth century.
(Attribution unknown)
Montpellier is an old city in southern France. It stands about halfway between Marseille and the Spanish border along the Mediterranean Sea (strategically located slightly inland to avoid pirates). First documented in the tenth century, it is one of very few French cities that developed without the influence of ancient Roman occupation; it is a pure product of the local region. It became a center of intellectual learning and attracted students from throughout Europe. Around it sprung a number of supporting arts not the least of which was glassmaking. Once famous for its fine glassware, today this centuries long heritage is all but forgotten, yet when we dig into the literature, we find a surprise connection to one of the oldest legends in the history of glass.

Since before the Renaissance, Montpellier was an established center for medical and legal education, a strong tradition that continues at the university there; today, it houses the oldest running medical school in the world. This prestigious institution "was founded perhaps by people trained in the Spanish medical schools; it is certain that, as early as 1137, there were excellent physicians at Montpellier University." [1] In 1529, Nostradamus entered to study for a doctorate in medicine, but shortly thereafter, he was expelled when it was discovered that he previously worked as an apothecary; a 'manual' skill that was banned by the school's rules of conduct.

Paradoxically, these impugned 'manual' arts account for some the region's more intriguing activity. Along with medicine, the area became known for the production of paint pigments, for glassmaking and finally for the practice of alchemy. All of these turn out to be closely related to each other, but perhaps not obviously so. Throughout the Renaissance, apothecaries were responsible for a wide range of distillations and extracts used by physicians to treat disease. They were also the de facto suppliers of pigments and other fine art supplies and even sourced some of the materials for glassmaking. Glassmakers often relied on painters to embellish their products, painters used ground glass in their pigments and apothecaries needed glassmakers to produce the flasks, beakers and other alchemical equipment required for their profession.

An anonymous Montpellier manuscript of the fourteenth century, called the Liber diversarum arcium [Book of Various Arts], offers us one of the most complete guides to the production of pigments to have survived from that period. [2] Another, later writing of the sixteenth century offers an extensive collection of glassmaking recipies brought to Montpellier from Venice. This one is titled Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536 [Recipes to make colored glasses and enamels of every kind as in Murano, 1536]. [3]

Local history points to the town of Claret just north of Montpellier as the seat of regional glassmaking. Beginning in 1290, the oak forests on the Causse de l'Orthus attracted glassmakers and their families. "So maybe the oaks got used for fuel. (A 'causse' is a geological term for a limestone plateau.) [also a material of glassmaking] At any rate, the glassmakers were ennobled by the King and formed a guild of premium glassmakers whose wares were sold all over Europe from the market at Sommières." [4]

In the early seventeenth century, Pierre-Jean Fabre (1588-1658) studied medicine at Montpellier where he discovered the works of Paracelsus, to which he became a devotee. [5] After securing a medical degree, he returned to the nearby town of his birth, Castelnaudary, to work as a doctor. Eventually, he was awarded the status of "Royal Physician" by Louis XIII, probably for his work on treating victims of the plague with chemical preparations. [6]

Fabre's first book, of a total canon numbering sixteen volumes, was on the subject of alchemy and medicine titled "Palladium spagyricum" 1624. [7] The book, written in Latin, contains advice on the transmutation of metals, turning water into "good wine" and elixirs to cure all disease. It contains one recipe that is of particular interest on the subject of glassmaking; a malleable form of glass, known in legend since the Roman Empire as Vitrum Flexile.

See my next post to take a closer look at Fabre's specific recipe for a glass that is malleable at room temperature and trace a bit of the legend's history.

[1] Wikipedia, “University of Montpellier” https://en.wikipedia.org/wiki/University_of_Montpellier.
[2] Mark Clarke: Mediaeval Painters' Materials and Techniques: The Montpellier Liber diversarum arcium (London: Archetype Publications, 2011).
[3] Montpellier 1536, MS. H. 486: Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536, Bibliothèque de l'Ecole de Médecine de Montpellier, see also Zecchin 1987, v.1 p 247-276. Although the manuscript is dated 1536 it is probably copied from much earlier Venetian sources.
 [4] Ed Ward, Blog: City on a Hill, 1 Nov. 2010 post “Where the Glass-Blowers Were.” http://wardinfrance.blogspot.com/2010/11/where-glass-blowers-were.html . Also see Halle du Verre regional glass museum website http://www.cc-grandpicsaintloup.fr/-Halle-du-verre-.html .
[5] Paracelsus (1493-1541) was a Swiss born physician and alchemist who looked to nature rather than ancient texts for remedies to disease. He was widely condemned durring his lifetime but became very popular after his manuscripts were printed in the late sixteenth century.
[6] The definitive reference on Fabre is Bernard Joly: La rationalité de l'alchimie au XVIIe siècle (France: Vrin, 1992), pp. 35-50. A good English treatment can be found in Allen George Debus: The French Paracelsians: The Chemical Challenge to Medical and Scientific Tradition in Early Modern France (Cambridge: Cambridge University Press, 2002) pp, 75, 76.
[7] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, notably by William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.

Wednesday, September 25, 2019

Vitrum Flexile [Flexible Glass]

Roman Emperor Tiberius - Glass paste cameo
 c 20ACE by "Herophilos, Son of Dioskurides"
In the first century CE, references appear in the literature for a malleable form of glass --that is to say flexible-- the method for which is reported as lost. This 'vitrum flexile' was a material that supposedly could be worked with a hammer like metal; not brittle but plastic, yet retaining the other favorable properties of glass. In the ancient world, historians Strabo (c. 63 BCE–24 CE), Pliny (c. 23–79 CE), Petronius (c. 27–66 CE) and others recount the story of a hapless artisan who brought his great discovery to Roman emperor Tiberius. Fearing the devaluation of his wealth, the emperor had the glassmaker executed on the spot and his workshop destroyed. The implication being that the inestimable value of a malleable glass would crash the markets for gold and silver. [1]

Since then, the legend has resurfaced in various forms, notably at periods in history of technological upheaval; times when innovative knowledge threatened to 'disrupt' the established order. One incarnation has the sophy of Persia gifting a set of malleable drinking glasses to the king of Spain, Philip III, around 1610. Just then, new trade deals with the Middle East rattled the European economy and Venetian glass craftsmen fanned out through Europe, disrupting local glass furnaces and guilds with their superior techniques. [2] Another version tells of a French sculptor bringing his malleable glass-work to Cardinal Richelieu (1585-1642), of Dumas' Three Musketeers fame. According to the story, that particular artisan’s reward was life in prison. The tale takes place in a tumultuous political period in French history and appears in print at the dawn of the so-called industrial revolution. [3]

Chronologically, this last story aligns nicely with the publication, in southern France, of a Latin book of alchemical recipes by royal physician Pierre-Jean Fabre (1588-1658). Contained in his volume is a prescription for a malleable form of glass, presumably the fabled vitrum flexile. Fabre's book was titled Palladium Spagyricum, 1624. [4] Spagyricum is a reference to spagyrics, the specific brand of chemistry practiced by sixteenth century alchemist-physician Paracelsus. Palladium translates to 'protector' or 'savior'. As an aside, it is interesting to note that Fabre developed an elaborate philosophy which integrated chemistry as a 'sacrament' to Catholic theology, but that is a story for another day.

In 1685, Fabre's recipes were nicely translated into English and tucked into the end of a book otherwise devoted to the art of drawing, by William Salmon [5]. Here is the full recipe "To Make Malleable Glass" as rendered in Salmon's book:

I.        Take oyl of Luna, twenty drachms: oyl of Mercury, or its water seven times rectified, one pound: mix them together and distill them.
II.      Repeat this distillation till the oleum Lunae rises with the water of Mercury in distillation. 
III.     Distill this water again until it is fixed, and converted into a fixed oyl, and this repeat four times. 
IV.     In the fourth time the oyl of Luna is fixed with the oyl of Mercury, so that they render glass malleable; for so great is the viscosity in your oyls, that it removes the brittleness of the glass, and so leaves it of a malleable temper. 
V.      The reason is, because that the radical moisture of the glass is multiplied by the radical moisture of the metals. Which is plentiful and turgent or swelling in the oyls of Luna and Mercury. 
VI.     And if [in] this oyl made volatile, diamonds should be dissolved, and then digested into a fixt oyl, it would transmute all glass into diamonds, only by projecting this oyl onto melted glass. 
VII.   There are also other precious stones comprehended within this oyl, when it is made volatile, and digested, and fixed again by digestion continually for the space of a year. 
VIII.  Also this oyl can turn glass into precious stones of any kind whatsoever, if therein (being made volatile) precious stones of the same kind have been dissolved, and digested with it into a fixed oyl. 
IX.     For as metals are included in their fixed oyls: so are precious stones in theirs, as Raymundus Lullius doth witness in many places; the which thing we shall teach you in the following chapter. 
 Elsewhere in the book, it is explained that 'oyl of Luna' is silver dissolved in acid, and 'oyl of Mercury' is a sublimation of mercury and saltpeter. [6] From a purely technical standpoint, the formula would have been regarded credible by 17th century and earlier practitioners in that both mercury and silver were successfully used as additives to glass and they do integrate into the matrix. Notably, Antonio Neri used both of them in his chalcedony glass. In Neri's case he was using these metals to produce color, although he does not attribute specific tints to the ingredients. Under some circumstances, silver is known to produce an attractive blue. It should also be noted that Renaissance glassmakers used similar silver-mercury formulas to produce the reflective layer on finished glass mirrors, in a process that resembled gilding. They formed what was known as "mercury glass." It is not beyond the pale to speculate that experiments would have been conducted by alchemists to add such concoctions directly to the glass melt. In the end, though, there is no indication that these additives would produce a malleable glass. Last, we should note that prolonged exposure to mercury vapor causes irreversable neurological and organ damage. It undoubetly contributed to the demise of alchemists, gilders, milliners and many others who worked with it throughout history. 

As far as I am aware, this is the first example of a specific recipe for malleable glass uncovered in the literature. If nothing else, it is an important marker for further research into the history of glassmaking.


[1] Strabo: Geography, v. 8; Pliny: Naturalis Historia XXXVI.lxvi.195; Petronius: Satyricon 50.7; Also recounted by Casius Dio (c.150–235 CE): Historia Romana 57.21.7; Isidore of Seville (c. 560–636 CE): Etymologiae XVI.16.6, ‘De vitro’; Suetonius; Ibn Abd Alhokin; John of Sailsbury.
[2] Knolles, Grimstone, Johnson: Richard Knolles' The General Historie of the Turkes (London: Adam Islip, 1621).
[3] Neri 1697 (Introduction). A French translation of Florentine glassmaker Antonio Neri’s 1612 book L’Arte Vetraria [The art of making glass] by Jean Haudicquer de Blancourt. Also see my earlier post here http://www.conciatore.org/2014/07/flexible-glass-reprise.html .
[4] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, see note [5].
[5] William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.
[6] To more adventurous readers: DO NOT TRY THIS AT HOME, or anywhere else, ever. Vaporized mercury is a powerful neurotoxin. Small amounts can cause permanent brain damage and multiple organ failure. Furthermore, this recipe uses powerful acids and nitrates, which are extremely dangerous even in a controlled laboratory setting. Even if you have little regard for your own health and safety, consider those around you; this includes loved ones, family, children, pets, neighbors and the emergency workers who will inevitably be left to clean up your mess.

Monday, September 23, 2019

The Glass of Montpellier

Montpellier, France, in the seventeenth century.
(Attribution unknown)
Montpellier is an old city in southern France. It stands about halfway between Marseille and the Spanish border along the Mediterranean Sea (strategically located slightly inland to avoid pirates). First documented in the tenth century, it is one of very few French cities that developed without the influence of ancient Roman occupation; it is a pure product of the local region. It became a center of intellectual learning and attracted students from throughout Europe. Around it sprung a number of supporting arts not the least of which was glassmaking. Once famous for its fine glassware, today this centuries long heritage is all but forgotten, yet when we dig into the literature, we find a surprise connection to one of the oldest legends in the history of glass.

Since before the Renaissance, Montpellier was an established center for medical and legal education, a strong tradition that continues at the university there; today, it houses the oldest running medical school in the world. This prestigious institution "was founded perhaps by people trained in the Spanish medical schools; it is certain that, as early as 1137, there were excellent physicians at Montpellier University." [1] In 1529, Nostradamus entered to study for a doctorate in medicine, but shortly thereafter, he was expelled when it was discovered that he previously worked as an apothecary; a 'manual' skill that was banned by the school's rules of conduct.

Paradoxically, these impugned 'manual' arts account for some the region's more intriguing activity. Along with medicine, the area became known for the production of paint pigments, for glassmaking and finally for the practice of alchemy. All of these turn out to be closely related to each other, but perhaps not obviously so. Throughout the Renaissance, apothecaries were responsible for a wide range of distillations and extracts used by physicians to treat disease. They were also the de facto suppliers of pigments and other fine art supplies and even sourced some of the materials for glassmaking. Glassmakers often relied on painters to embellish their products, painters used ground glass in their pigments and apothecaries needed glassmakers to produce the flasks, beakers and other alchemical equipment required for their profession.

An anonymous Montpellier manuscript of the fourteenth century, called the Liber diversarum arcium [Book of Various Arts], offers us one of the most complete guides to the production of pigments to have survived from that period. [2] Another, later writing of the sixteenth century offers an extensive collection of glassmaking recipies brought to Montpellier from Venice. This one is titled Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536 [Recipes to make colored glasses and enamels of every kind as in Murano, 1536]. [3]

Local history points to the town of Claret just north of Montpellier as the seat of regional glassmaking. Beginning in 1290, the oak forests on the Causse de l'Orthus attracted glassmakers and their families. "So maybe the oaks got used for fuel. (A 'causse' is a geological term for a limestone plateau.) [also a material of glassmaking] At any rate, the glassmakers were ennobled by the King and formed a guild of premium glassmakers whose wares were sold all over Europe from the market at Sommières." [4]

In the early seventeenth century, Pierre-Jean Fabre (1588-1658) studied medicine at Montpellier where he discovered the works of Paracelsus, to which he became a devotee. [5] After securing a medical degree, he returned to the nearby town of his birth, Castelnaudary, to work as a doctor. Eventually, he was awarded the status of "Royal Physician" by Louis XIII, probably for his work on treating victims of the plague with chemical preparations. [6]

Fabre's first book, of a total canon numbering sixteen volumes, was on the subject of alchemy and medicine titled "Palladium spagyricum" 1624. [7] The book, written in Latin, contains advice on the transmutation of metals, turning water into "good wine" and elixirs to cure all disease. It contains one recipe that is of particular interest on the subject of glassmaking; a malleable form of glass, known in legend since the Roman Empire as Vitrum Flexile.

See my next post to take a closer look at Fabre's specific recipe for a glass that is malleable at room temperature and trace a bit of the legend's history.

[1] Wikipedia, “University of Montpellier” https://en.wikipedia.org/wiki/University_of_Montpellier.
[2] Mark Clarke: Mediaeval Painters' Materials and Techniques: The Montpellier Liber diversarum arcium (London: Archetype Publications, 2011).
[3] Montpellier 1536, MS. H. 486: Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536, Bibliothèque de l'Ecole de Médecine de Montpellier, see also Zecchin 1987, v.1 p 247-276. Although the manuscript is dated 1536 it is probably copied from much earlier Venetian sources.
 [4] Ed Ward, Blog: City on a Hill, 1 Nov. 2010 post “Where the Glass-Blowers Were.” http://wardinfrance.blogspot.com/2010/11/where-glass-blowers-were.html . Also see Halle du Verre regional glass museum website http://www.cc-grandpicsaintloup.fr/-Halle-du-verre-.html .
[5] Paracelsus (1493-1541) was a Swiss born physician and alchemist who looked to nature rather than ancient texts for remedies to disease. He was widely condemned durring his lifetime but became very popular after his manuscripts were printed in the late sixteenth century.
[6] The definitive reference on Fabre is Bernard Joly: La rationalité de l'alchimie au XVIIe siècle (France: Vrin, 1992), pp. 35-50. A good English treatment can be found in Allen George Debus: The French Paracelsians: The Chemical Challenge to Medical and Scientific Tradition in Early Modern France (Cambridge: Cambridge University Press, 2002) pp, 75, 76.
[7] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, notably by William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.

Wednesday, January 16, 2019

The Glass of Montpellier

Montpellier, France, in the seventeenth century.
(Attribution unknown)
Montpellier is an old city in southern France. It stands about halfway between Marseille and the Spanish border along the Mediterranean Sea (strategically located slightly inland to avoid pirates). First documented in the tenth century, it is one of very few French cities that developed without the influence of ancient Roman occupation; it is a pure product of the local region. It became a center of intellectual learning and attracted students from throughout Europe. Around it sprung a number of supporting arts not the least of which was glassmaking. Once famous for its fine glassware, today this centuries long heritage is all but forgotten, yet when we dig into the literature, we find a surprise connection to one of the oldest legends in the history of glass.

Since before the Renaissance, Montpellier was an established center for medical and legal education, a strong tradition that continues at the university there; today, it houses the oldest running medical school in the world. This prestigious institution "was founded perhaps by people trained in the Spanish medical schools; it is certain that, as early as 1137, there were excellent physicians at Montpellier University." [1] In 1529, Nostradamus entered to study for a doctorate in medicine, but shortly thereafter, he was expelled when it was discovered that he previously worked as an apothecary; a 'manual' skill that was banned by the school's rules of conduct.

Paradoxically, these impugned 'manual' arts account for some the region's more intriguing activity. Along with medicine, the area became known for the production of paint pigments, for glassmaking and finally for alchemy. All of these turn out to be closely related to each other, but perhaps not obviously so. Throughout the Renaissance, apothecaries were responsible for a wide range of distillations and extracts used by physicians to treat disease. They were also the de facto suppliers of pigments and other fine art supplies and even sourced some of the materials for glassmaking. Glassmakers often relied on painters to embellish their products, painters used ground glass in their pigments and apothecaries needed glassmakers to produce the flasks, beakers and other alchemical equipment required for their profession.

An anonymous Montpellier manuscript of the fourteenth century, called the Liber diversarum arcium [Book of Various Arts], offers us one of the most complete guides to the production of pigments to have survived from that period. [2] Another, later writing of the sixteenth century offers an extensive collection of glassmaking recipies brought to Montpellier from Venice. This one is titled Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536 [Recipes to make colored glasses and enamels of every kind as in Murano, 1536]. [3]

Local history points to the town of Claret just north of Montpellier as the seat of regional glassmaking. Beginning in 1290, the oak forests on the Causse de l'Orthus attracted glassmakers and their families. "So maybe the oaks got used for fuel. (A 'causse' is a geological term for a limestone plateau.) [also a material of glassmaking] At any rate, the glassmakers were ennobled by the King and formed a guild of premium glassmakers whose wares were sold all over Europe from the market at Sommières." [4]

In the early seventeenth century, Pierre-Jean Fabre (1588-1658) studied medicine at Montpellier where he discovered the works of Paracelsus, to which he became a devotee. [5] After securing a medical degree, he returned to the nearby town of his birth, Castelnaudary, to work as a doctor. Eventually, he was awarded the status of "Royal Physician" by Louis XIII, probably for his work on treating victims of the plague with chemical preparations. [6]

Fabre's first book, of a total canon numbering sixteen volumes, was on the subject of alchemy and medicine titled "Palladium spagyricum" 1624. [7] The book, written in Latin, contains advice on the transmutation of metals, turning water into "good wine" and elixirs to cure all disease. It contains one recipe that is of particular interest on the subject of glassmaking; a malleable form of glass, known in legend since the Roman Empire as Vitrum Flexile.

See my previous post to take a closer look at Fabre's specific recipe for a glass that is malleable at room temperature and trace a bit of the legend's history.

[1] Wikipedia, “University of Montpellier” https://en.wikipedia.org/wiki/University_of_Montpellier.
[2] Mark Clarke: Mediaeval Painters' Materials and Techniques: The Montpellier Liber diversarum arcium (London: Archetype Publications, 2011).
[3] Montpellier 1536, MS. H. 486: Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536, Bibliothèque de l'Ecole de Médecine de Montpellier, see also Zecchin 1987, v.1 p 247-276. Although the manuscript is dated 1536 it is probably copied from much earlier Venetian sources.
 [4] Ed Ward, Blog: City on a Hill, 1 Nov. 2010 post “Where the Glass-Blowers Were.” http://wardinfrance.blogspot.com/2010/11/where-glass-blowers-were.html . Also see Halle du Verre regional glass museum website http://www.cc-grandpicsaintloup.fr/-Halle-du-verre-.html .
[5] Paracelsus (1493-1541) was a Swiss born physician and alchemist who looked to nature rather than ancient texts for remedies to disease. He was widely condemned durring his lifetime but became very popular after his manuscripts were printed in the late sixteenth century.
[6] The definitive reference on Fabre is Bernard Joly: La rationalité de l'alchimie au XVIIe siècle (France: Vrin, 1992), pp. 35-50. A good English treatment can be found in Allen George Debus: The French Paracelsians: The Chemical Challenge to Medical and Scientific Tradition in Early Modern France (Cambridge: Cambridge University Press, 2002) pp, 75, 76.
[7] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, notably by William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.

Monday, January 14, 2019

Vitrum Flexile

Roman Emperor Tiberius - Glass paste cameo
 c 20ACE by "Herophilos, Son of Dioskurides"
In the first century CE, references appear in the literature for a malleable form of glass --that is to say flexible-- the method for which is reported as lost. This 'vitrum flexile' was a material that supposedly could be worked with a hammer like metal; not brittle but plastic, yet retaining the other favorable properties of glass. In the ancient world, historians Strabo (c. 63 BCE–24 CE), Pliny (c. 23–79 CE), Petronius (c. 27–66 CE) and others recount the story of a hapless artisan who brought his great discovery to Roman emperor Tiberius. Fearing the devaluation of his wealth, the emperor had the glassmaker executed on the spot and his workshop destroyed. The implication being that the inestimable value of a malleable glass would crash the markets for gold and silver. [1]

Since then, the legend has resurfaced in various forms, notably at periods in history of technological upheaval; times when innovative knowledge threatened to 'disrupt' the established order. One incarnation has the sophy of Persia gifting a set of malleable drinking glasses to the king of Spain, Philip III, around 1610. Just then, new trade deals with the Middle East rattled the European economy and Venetian glass craftsmen fanned out through Europe, disrupting local glass furnaces and guilds with their superior techniques. [2] Another version tells of a French sculptor bringing his malleable glass-work to Cardinal Richelieu (1585-1642), of Dumas' Three Musketeers fame. According to the story, that particular artisan’s reward was life in prison. The tale takes place in a tumultuous political period in French history and appears in print at the dawn of the so-called industrial revolution. [3]

Chronologically, this last story aligns nicely with the publication, in southern France, of a Latin book of alchemical recipes by royal physician Pierre-Jean Fabre (1588-1658). Contained in his volume is a prescription for a malleable form of glass, presumably the fabled vitrum flexile. Fabre's book was titled Palladium Spagyricum, 1624. [4] Spagyricum is a reference to spagyrics, the specific brand of chemistry practiced by sixteenth century alchemist-physician Paracelsus. Palladium translates to 'protector' or 'savior'. As an aside, it is interesting to note that Fabre developed an elaborate philosophy which integrated chemistry as a 'sacrament' to Catholic theology, but that is a story for another day.

In 1685, Fabre's recipes were nicely translated into English and tucked into the end of a book otherwise devoted to the art of drawing, by William Salmon [5]. Here is the full recipe "To Make Malleable Glass" as rendered in Salmon's book:

I.        Take oyl of Luna, twenty drachms: oyl of Mercury, or its water seven times rectified, one pound: mix them together and distill them.
II.      Repeat this distillation till the oleum Lunae rises with the water of Mercury in distillation. 
III.     Distill this water again until it is fixed, and converted into a fixed oyl, and this repeat four times. 
IV.     In the fourth time the oyl of Luna is fixed with the oyl of Mercury, so that they render glass malleable; for so great is the viscosity in your oyls, that it removes the brittleness of the glass, and so leaves it of a malleable temper. 
V.      The reason is, because that the radical moisture of the glass is multiplied by the radical moisture of the metals. Which is plentiful and turgent or swelling in the oyls of Luna and Mercury. 
VI.     And if [in] this oyl made volatile, diamonds should be dissolved, and then digested into a fixt oyl, it would transmute all glass into diamonds, only by projecting this oyl onto melted glass. 
VII.   There are also other precious stones comprehended within this oyl, when it is made volatile, and digested, and fixed again by digestion continually for the space of a year. 
VIII.  Also this oyl can turn glass into precious stones of any kind whatsoever, if therein (being made volatile) precious stones of the same kind have been dissolved, and digested with it into a fixed oyl. 
IX.     For as metals are included in their fixed oyls: so are precious stones in theirs, as Raymundus Lullius doth witness in many places; the which thing we shall teach you in the following chapter. 
 Elsewhere in the book, it is explained that 'oyl of Luna' is silver dissolved in acid, and 'oyl of Mercury' is a sublimation of mercury and saltpeter. [6] From a purely technical standpoint, the formula would have been regarded credible by 17th century and earlier practitioners in that both mercury and silver were successfully used as additives to glass and they do integrate into the matrix. Notably, Antonio Neri used both of them in his chalcedony glass. In Neri's case he was using these metals to produce color, although he does not attribute specific tints to the ingredients. Under some circumstances, silver is known to produce an attractive blue. It should also be noted that Renaissance glassmakers used similar silver-mercury formulas to produce the reflective layer on finished glass mirrors, in a process that resembled gilding. They formed what was known as "mercury glass." It is not beyond the pale to speculate that experiments would have been conducted by alchemists to add such concoctions directly to the glass melt. In the end, though, there is no indication that these additives would produce a malleable glass. Last, we should note that prolonged exposure to mercury vapor causes irreversable neurological and organ damage. It undoubetly contributed to the demise of alchemists, gilders, milliners and many others who worked with it throughout history. 

As far as I am aware, this is the first example of a specific recipe for malleable glass uncovered in the literature. If nothing else, it is an important marker for further research into the history of glassmaking.


[1] Strabo: Geography, v. 8; Pliny: Naturalis Historia XXXVI.lxvi.195; Petronius: Satyricon 50.7; Also recounted by Casius Dio (c.150–235 CE): Historia Romana 57.21.7; Isidore of Seville (c. 560–636 CE): Etymologiae XVI.16.6, ‘De vitro’; Suetonius; Ibn Abd Alhokin; John of Sailsbury.
[2] Knolles, Grimstone, Johnson: Richard Knolles' The General Historie of the Turkes (London: Adam Islip, 1621).
[3] Neri 1697 (Introduction). A French translation of Florentine glassmaker Antonio Neri’s 1612 book L’Arte Vetraria [The art of making glass] by Jean Haudicquer de Blancourt. Also see my earlier post here http://www.conciatore.org/2014/07/flexible-glass-reprise.html .
[4] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, see note [5].
[5] William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.
[6] To more adventurous readers: DO NOT TRY THIS AT HOME, or anywhere else, ever. Vaporized mercury is a powerful neurotoxin. Small amounts can cause permanent brain damage and multiple organ failure. Furthermore, this recipe uses powerful acids and nitrates, which are extremely dangerous even in a controlled laboratory setting. Even if you have little regard for your own health and safety, consider those around you; this includes loved ones, family, children, pets, neighbors and the emergency workers who will inevitably be left to clean up your mess.

Friday, April 13, 2018

The Glass of Montpellier

Montpellier, France, in the seventeenth century.
(Attribution unknown)
Montpellier is an old city in southern France. It stands about halfway between Marseille and the Spanish border along the Mediterranean Sea (strategically located slightly inland to avoid pirates). First documented in the tenth century, it is one of very few French cities that developed without the influence of ancient Roman occupation; it is a pure product of the local region. It became a center of intellectual learning and attracted students from throughout Europe. Around it sprung a number of supporting arts not the least of which was glassmaking. Once famous for its fine glassware, today this centuries long heritage is all but forgotten, yet when we dig into the literature, we find a surprise connection to one of the oldest legends in the history of glass.

Since before the Renaissance, Montpellier was an established center for medical and legal education, a strong tradition that continues at the university there; today, it houses the oldest running medical school in the world. This prestigious institution "was founded perhaps by people trained in the Spanish medical schools; it is certain that, as early as 1137, there were excellent physicians at Montpellier University." [1] In 1529, Nostradamus entered to study for a doctorate in medicine, but shortly thereafter, he was expelled when it was discovered that he previously worked as an apothecary; a 'manual' skill that was banned by the school's rules of conduct.

Paradoxically, these impugned 'manual' arts account for some the region's more intriguing activity. Along with medicine, the area became known for the production of paint pigments, for glassmaking and finally for alchemy. All of these turn out to be closely related to each other, but perhaps not obviously so. Throughout the Renaissance, apothecaries were responsible for a wide range of distillations and extracts used by physicians to treat disease. They were also the de facto suppliers of pigments and other fine art supplies and even sourced some of the materials for glassmaking. Glassmakers often relied on painters to embellish their products, painters used ground glass in their pigments and apothecaries needed glassmakers to produce the flasks, beakers and other alchemical equipment required for their profession.

An anonymous Montpellier manuscript of the fourteenth century, called the Liber diversarum arcium [Book of Various Arts], offers us one of the most complete guides to the production of pigments to have survived from that period. [2] Another, later writing of the sixteenth century offers an extensive collection of glassmaking recipies brought to Montpellier from Venice. This one is titled Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536 [Recipes to make colored glasses and enamels of every kind as in Murano, 1536]. [3]

Local history points to the town of Claret just north of Montpellier as the seat of regional glassmaking. Beginning in 1290, the oak forests on the Causse de l'Orthus attracted glassmakers and their families. "So maybe the oaks got used for fuel. (A 'causse' is a geological term for a limestone plateau.) [also a material of glassmaking] At any rate, the glassmakers were ennobled by the King and formed a guild of premium glassmakers whose wares were sold all over Europe from the market at Sommières." [4]

In the early seventeenth century, Pierre-Jean Fabre (1588-1658) studied medicine at Montpellier where he discovered the works of Paracelsus, to which he became a devotee. [5] After securing a medical degree, he returned to the nearby town of his birth, Castelnaudary, to work as a doctor. Eventually, he was awarded the status of "Royal Physician" by Louis XIII, probably for his work on treating victims of the plague with chemical preparations. [6]

Fabre's first book, of a total canon numbering sixteen volumes, was on the subject of alchemy and medicine titled "Palladium spagyricum" 1624. [7] The book, written in Latin, contains advice on the transmutation of metals, turning water into "good wine" and elixirs to cure all disease. It contains one recipe that is of particular interest on the subject of glassmaking; a malleable form of glass, known in legend since the Roman Empire as Vitrum Flexile.

See my previous post to take a closer look at Fabre's specific recipe for a glass that is malleable at room temperature and trace a bit of the legend's history.

[1] Wikipedia, “University of Montpellier” https://en.wikipedia.org/wiki/University_of_Montpellier.
[2] Mark Clarke: Mediaeval Painters' Materials and Techniques: The Montpellier Liber diversarum arcium (London: Archetype Publications, 2011).
[3] Montpellier 1536, MS. H. 486: Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536, Bibliothèque de l'Ecole de Médecine de Montpellier, see also Zecchin 1987, v.1 p 247-276. Although the manuscript is dated 1536 it is probably copied from much earlier Venetian sources.
 [4] Ed Ward, Blog: City on a Hill, 1 Nov. 2010 post “Where the Glass-Blowers Were.” http://wardinfrance.blogspot.com/2010/11/where-glass-blowers-were.html . Also see Halle du Verre regional glass museum website http://www.cc-grandpicsaintloup.fr/-Halle-du-verre-.html .
[5] Paracelsus (1493-1541) was a Swiss born physician and alchemist who looked to nature rather than ancient texts for remedies to disease. He was widely condemned durring his lifetime but became very popular after his manuscripts were printed in the late sixteenth century.
[6] The definitive reference on Fabre is Bernard Joly: La rationalité de l'alchimie au XVIIe siècle (France: Vrin, 1992), pp. 35-50. A good English treatment can be found in Allen George Debus: The French Paracelsians: The Chemical Challenge to Medical and Scientific Tradition in Early Modern France (Cambridge: Cambridge University Press, 2002) pp, 75, 76.
[7] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, notably by William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.

Wednesday, April 11, 2018

Vitrum Flexile

Roman Emperor Tiberius - Glass paste cameo
 c 20ACE by "Herophilos, Son of Dioskurides"
In the first century CE, references appear in the literature for a malleable form of glass --that is to say flexible-- the method for which is reported as lost. This 'vitrum flexile' was a material that supposedly could be worked with a hammer like metal; not brittle but plastic, yet retaining the other favorable properties of glass. In the ancient world, historians Strabo (c. 63 BCE–24 CE), Pliny (c. 23–79 CE), Petronius (c. 27–66 CE) and others recount the story of a hapless artisan who brought his great discovery to Roman emperor Tiberius. Fearing the devaluation of his wealth, the emperor had the glassmaker executed on the spot and his workshop destroyed. The implication being that the inestimable value of a malleable glass would crash the markets for gold and silver. [1]

Since then, the legend has resurfaced in various forms, notably at periods in history of technological upheaval; times when innovative knowledge threatened to 'disrupt' the established order. One incarnation has the sophy of Persia gifting a set of malleable drinking glasses to the king of Spain, Philip III, around 1610. Just then, new trade deals with the Middle East rattled the European economy and Venetian glass craftsmen fanned out through Europe, disrupting local glass furnaces and guilds with their superior techniques. [2] Another version tells of a French sculptor bringing his malleable glass-work to Cardinal Richelieu (1585-1642), of Dumas' Three Musketeers fame. According to the story, that particular artisan’s reward was life in prison. The tale takes place in a tumultuous political period in French history and appears in print at the dawn of the so-called industrial revolution. [3]

Chronologically, this last story aligns nicely with the publication, in southern France, of a Latin book of alchemical recipes by royal physician Pierre-Jean Fabre (1588-1658). Contained in his volume is a prescription for a malleable form of glass, presumably the fabled vitrum flexile. Fabre's book was titled Palladium Spagyricum, 1624. [4] Spagyricum is a reference to spagyrics, the specific brand of chemistry practiced by sixteenth century alchemist-physician Paracelsus. Palladium translates to 'protector' or 'savior'. As an aside, it is interesting to note that Fabre developed an elaborate philosophy which integrated chemistry as a 'sacrament' to Catholic theology, but that is a story for another day.

In 1685, Fabre's recipes were nicely translated into English and tucked into the end of a book otherwise devoted to the art of drawing, by William Salmon [5]. Here is the full recipe "To Make Malleable Glass" as rendered in Salmon's book:

I.        Take oyl of Luna, twenty drachms: oyl of Mercury, or its water seven times rectified, one pound: mix them together and distill them.
II.      Repeat this distillation till the oleum Lunae rises with the water of Mercury in distillation. 
III.     Distill this water again until it is fixed, and converted into a fixed oyl, and this repeat four times. 
IV.     In the fourth time the oyl of Luna is fixed with the oyl of Mercury, so that they render glass malleable; for so great is the viscosity in your oyls, that it removes the brittleness of the glass, and so leaves it of a malleable temper. 
V.      The reason is, because that the radical moisture of the glass is multiplied by the radical moisture of the metals. Which is plentiful and turgent or swelling in the oyls of Luna and Mercury. 
VI.     And if [in] this oyl made volatile, diamonds should be dissolved, and then digested into a fixt oyl, it would transmute all glass into diamonds, only by projecting this oyl onto melted glass. 
VII.   There are also other precious stones comprehended within this oyl, when it is made volatile, and digested, and fixed again by digestion continually for the space of a year. 
VIII.  Also this oyl can turn glass into precious stones of any kind whatsoever, if therein (being made volatile) precious stones of the same kind have been dissolved, and digested with it into a fixed oyl. 
IX.     For as metals are included in their fixed oyls: so are precious stones in theirs, as Raymundus Lullius doth witness in many places; the which thing we shall teach you in the following chapter. 
 Elsewhere in the book, it is explained that 'oyl of Luna' is silver dissolved in acid, and 'oyl of Mercury' is a sublimation of mercury and saltpeter. [6] From a purely technical standpoint, the formula would have been regarded credible by 17th century and earlier practitioners in that both mercury and silver were successfully used as additives to glass and they do integrate into the matrix. Notably, Antonio Neri used both of them in his chalcedony glass. In Neri's case he was using these metals to produce color, although he does not attribute specific tints to the ingredients. Under some circumstances, silver is known to produce an attractive blue. It should also be noted that Renaissance glassmakers used similar silver-mercury formulas to produce the reflective layer on finished glass mirrors, in a process that resembled gilding. They formed what was known as "mercury glass." It is not beyond the pale to speculate that experiments would have been conducted by alchemists to add such concoctions directly to the glass melt. In the end, though, there is no indication that these additives would produce a malleable glass. Last, we should note that prolonged exposure to mercury vapor causes irreversable neurological and organ damage. It undoubetly contributed to the demise of alchemists, gilders, milliners and many others who worked with it throughout history. 

As far as I am aware, this is the first example of a specific recipe for malleable glass uncovered in the literature. If nothing else, it is an important marker for further research into the history of glassmaking.


[1] Strabo: Geography, v. 8; Pliny: Naturalis Historia XXXVI.lxvi.195; Petronius: Satyricon 50.7; Also recounted by Casius Dio (c.150–235 CE): Historia Romana 57.21.7; Isidore of Seville (c. 560–636 CE): Etymologiae XVI.16.6, ‘De vitro’; Suetonius; Ibn Abd Alhokin; John of Sailsbury.
[2] Knolles, Grimstone, Johnson: Richard Knolles' The General Historie of the Turkes (London: Adam Islip, 1621).
[3] Neri 1697 (Introduction). A French translation of Florentine glassmaker Antonio Neri’s 1612 book L’Arte Vetraria [The art of making glass] by Jean Haudicquer de Blancourt. Also see my earlier post here http://www.conciatore.org/2014/07/flexible-glass-reprise.html .
[4] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, see note [5].
[5] William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.
[6] To more adventurous readers: DO NOT TRY THIS AT HOME, or anywhere else, ever. Vaporized mercury is a powerful neurotoxin. Small amounts can cause permanent brain damage and multiple organ failure. Furthermore, this recipe uses powerful acids and nitrates, which are extremely dangerous even in a controlled laboratory setting. Even if you have little regard for your own health and safety, consider those around you; this includes loved ones, family, children, pets, neighbors and the emergency workers who will inevitably be left to clean up your mess.

Friday, June 23, 2017

Montpellier

Montpellier, France, in the seventeenth century.
(Attribution unknown)
Montpellier is an old city in southern France. It stands about halfway between Marseille and the Spanish border along the Mediterranean Sea (strategically located slightly inland to avoid pirates). First documented in the tenth century, it is one of very few French cities that developed without the influence of ancient Roman occupation; it is a pure product of the local region. It became a center of intellectual learning and attracted students from throughout Europe. Around it sprung a number of supporting arts not the least of which was glassmaking. Once famous for its fine glassware, today this centuries long heritage is all but forgotten, yet when we dig into the literature, we find a surprise connection to one of the oldest legends in the history of glass.

Since before the Renaissance, Montpellier was an established center for medical and legal education, a strong tradition that continues at the university there; today, it houses the oldest running medical school in the world. This prestigious institution "was founded perhaps by people trained in the Spanish medical schools; it is certain that, as early as 1137, there were excellent physicians at Montpellier University." [1] In 1529, Nostradamus entered to study for a doctorate in medicine, but shortly thereafter, he was expelled when it was discovered that he previously worked as an apothecary; a 'manual' skill that was banned by the school's rules of conduct.

Paradoxically, these impugned 'manual' arts account for some the region's more intriguing activity. Along with medicine, the area became known for the production of paint pigments, for glassmaking and finally for alchemy. All of these turn out to be closely related to each other, but perhaps not obviously so. Throughout the Renaissance, apothecaries were responsible for a wide range of distillations and extracts used by physicians to treat disease. They were also the de facto suppliers of pigments and other fine art supplies and even sourced some of the materials for glassmaking. Glassmakers often relied on painters to embellish their products, painters used ground glass in their pigments and apothecaries needed glassmakers to produce the flasks, beakers and other alchemical equipment required for their profession.

An anonymous Montpellier manuscript of the fourteenth century, called the Liber diversarum arcium [Book of Various Arts], offers us one of the most complete guides to the production of pigments to have survived from that period. [2] Another, later writing of the sixteenth century offers an extensive collection of glassmaking recipies brought to Montpellier from Venice. This one is titled Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536 [Recipes to make colored glasses and enamels of every kind as in Murano, 1536]. [3]

Local history points to the town of Claret just north of Montpellier as the seat of regional glassmaking. Beginning in 1290, the oak forests on the Causse de l'Orthus attracted glassmakers and their families. "So maybe the oaks got used for fuel. (A 'causse' is a geological term for a limestone plateau.) [also a material of glassmaking] At any rate, the glassmakers were ennobled by the King and formed a guild of premium glassmakers whose wares were sold all over Europe from the market at Sommières." [4]

In the early seventeenth century, Pierre-Jean Fabre (1588-1658) studied medicine at Montpellier where he discovered the works of Paracelsus, to which he became a devotee. [5] After securing a medical degree, he returned to the nearby town of his birth, Castelnaudary, to work as a doctor. Eventually, he was awarded the status of "Royal Physician" by Louis XIII, probably for his work on treating victims of the plague with chemical preparations. [6]

Fabre's first book, of a total canon numbering sixteen volumes, was on the subject of alchemy and medicine titled "Palladium spagyricum" 1624. [7] The book, written in Latin, contains advice on the transmutation of metals, turning water into "good wine" and elixirs to cure all disease. It contains one recipe that is of particular interest on the subject of glassmaking; a malleable form of glass, known in legend since the Roman Empire as Vitrum Flexile.

See my previous post to take a closer look at Fabre's specific recipe for a glass that is malleable at room temperature and trace a bit of the legend's history.

[1] Wikipedia, “University of Montpellier” https://en.wikipedia.org/wiki/University_of_Montpellier.
[2] Mark Clarke: Mediaeval Painters' Materials and Techniques: The Montpellier Liber diversarum arcium (London: Archetype Publications, 2011).
[3] Montpellier 1536, MS. H. 486: Recette per fare vetri colorati et smalti d’ogni sorte havute in Murano 1536, Bibliothèque de l'Ecole de Médecine de Montpellier, see also Zecchin 1987, v.1 p 247-276. Although the manuscript is dated 1536 it is probably copied from much earlier Venetian sources.
 [4] Ed Ward, Blog: City on a Hill, 1 Nov. 2010 post “Where the Glass-Blowers Were.” http://wardinfrance.blogspot.com/2010/11/where-glass-blowers-were.html . Also see Halle du Verre regional glass museum website http://www.cc-grandpicsaintloup.fr/-Halle-du-verre-.html .
[5] Paracelsus (1493-1541) was a Swiss born physician and alchemist who looked to nature rather than ancient texts for remedies to disease. He was widely condemned durring his lifetime but became very popular after his manuscripts were printed in the late sixteenth century.
[6] The definitive reference on Fabre is Bernard Joly: La rationalité de l'alchimie au XVIIe siècle (France: Vrin, 1992), pp. 35-50. A good English treatment can be found in Allen George Debus: The French Paracelsians: The Chemical Challenge to Medical and Scientific Tradition in Early Modern France (Cambridge: Cambridge University Press, 2002) pp, 75, 76.
[7] Pierre-Jean Fabre: Palladium spagyricum Petri Ioannis Fabri doctoris medici Monspeliensis ... (Toulouse: Bosc, 1624), p. 276. Later translated into several English editions, notably by William Salmon: Polygraphice: Or the Arts of Drawing, Engraving, Etching, Limming, Painting … (London: T. Passenger & T. Sawbridge, 1685), pp. 598, 599.